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GB/T 20884-2007 PDF English


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GB/T 20884-2007: PDF in English (GBT 20884-2007)

GB/T 20884-2007 NATIONAL STANDARD OF THE PEOPLE’S REPUBLIC OF CHINA ICS 67.180.20 X 31 Maltodextrin 麦芽糊精 ISSUED ON: FEBRUARY 02, 2007 IMPLEMENTED ON: DECEMBER 01, 2007 Issued by: General Administration of Quality Supervision, Inspection and Quarantine; Standardization Administration of PRC. Table of Contents Foreword ... 3  1 Scope ... 4  2 Normative references ... 4  3 Terms and definitions ... 4  4 Product classification ... 5  5 Requirements ... 5  6 Test method ... 5  7 Inspection rules ... 9  8 Marking, packaging, transportation and storage ... 11  Maltodextrin 1 Scope This standard specifies the terms and definitions, product classification, requirements, test methods, inspection rules, marking, packaging, transportation, storage of maltodextrin. This standard applies to maltodextrin. 2 Normative references The provisions in following documents become the provisions of this Standard through reference in this Standard. For the dated references, the subsequent amendments (excluding corrections) or revisions do not apply to this Standard; however, parties who reach an agreement based on this Standard are encouraged to study if the latest versions of these documents are applicable. For undated references, the latest edition of the referenced document applies. GB/T 191 Packaging - Pictorial marking for handling of goods (GB/T 191- 2000, eqv ISO 780:1997) GB/T 601 Chemical reagent - Preparations of standard volumetric solutions GB/T 6682-1992 Water for laboratory use - Specifications (neq ISO 3696:1987) GB 15203 Hygienic standard of corn sweetener GB/T 20885-2007 Glucose syrup 3 Terms and definitions The following terms and definitions apply to this standard. 3.1 Maltodextrin (MD) A starch derivative free of free starch made from starch or starchiness as a raw material, through enzymatical hydrolysis, refining, spray drying. 6.1.1 Appearance and color Take an appropriate amount of dextrin sample. Observe the color and form of the sample with naked eyes under natural light for impurities. 6.1.2 Odor Take 20 g of sample. Put it in a 100 mL grounded bottle. Add 50 mL of 50 °C warm water. Add cap. Shake it for 30 s. Decant the supernatant. Smell its odor. Record its odor characteristics. 6.1.3 Taste After rinsing mouth with clean water, take a small amount of sample int mouth. Taste it carefully. Record its taste characteristics. 6.2 DE value Determine it according to 6.3 in GB/T 20885-2007. 6.3 Moisture (direct drying method) 6.3.1 Instruments 6.3.1.1 Constant temperature drying oven: Temperature control accuracy ± 2 °C. 6.3.1.2 Analytical balance: Accuracy 0.1 mg. 6.3.1.3 Weighing dish: 50 mm x 30 mm. 6.3.1.4 Dryer: Use discoloration silica gel as the desiccant. 6.3.2 Analytical procedures Weigh 2 g of the sample (accurate to 0.0001 g) in a weighing dish that has been baked to constant weight. Put it in a 105 °C ± 2 °C constant temperature drying oven to dry it for 2 h. Move it into a desiccator to cool. Weigh it after 30 min. Put it in a constant temperature drying oven to bake for 1 h. Weigh it until reaching to constant weight. 6.3.3 Calculation of results The moisture of the sample is calculated according to formula (1). The value is expressed in %. Where: expressed in %. Where: X2 - Mass fraction of sample’s solubility, %; X1 - Mass fraction of the sample moisture, %; m2 - The mass of the weighing dish and quantitative filter paper plus filter residue after drying, in grams (g) m1 - The mass of the weighing dish and the quantitative filter paper, in grams (g) m - The mass of the sample, in grams (g). The result is expressed to one decimal place. 6.4.4 Precision The absolute difference between two independent determination results obtained under repeatability conditions shall not exceed 1% of the arithmetic mean. 6.5 pH 6.5.1 Instruments Acidity meter: Accuracy ±0.01 pH, equipped with glass electrode and calomel electrode (or composite electrode). 6.5.2 Analytical procedures 6.5.2.1 Commission and calibrate the acidity meter according to the instruction manual of the instrument. 6.5.2.2 Determination Weigh 20 g of the sample in a 50 mL beaker. Use 20 mL ~ 40 mL of neutral water which is removed of carbon dioxide to heat and dissolve it. Use distilled water to rinse the electrode probe. Use filter paper to gently absorb it dry. Then insert the electrode into the sample liquid to be measured. Adjust the temperature regulator, so that the temperature indicated by the instrument is the same as the temperature of the solution. Take the reading after it is stabilized. Where: A - The number of packaging units that shall be extracted, in bags. N - The total number of packaging units of the batch, in bags. 7.2.2 Extraction of uniform samples When sampling, use clean and dry sampling tools to insert two-half of the packaging bag. Take 100 g of sample from each bag. Quickly mix the extracted samples. Use the quartile method to reduce it. Then divide them into two 1000 mL grounded bottles that shall be clean and dry. Seal it. Attach labels. One bottle is used for testing and the other is retained for reference. 7.3 Exit-factory inspection 7.3.1 The finished products shall be inspected batch by batch by the inspection department before they leave the factory. 7.3.2 Exit-factory inspection items include: sensory requirements, moisture, DE value, pH, iodine test. 7.4 Type inspection Type inspection items are all items as specified in this standard. Under normal circumstances, type inspections are conducted every six months. In one of the following situations, type inspection shall also be carried out: a) When there are major changes in the original and auxiliary materials; b) Where there is change in critical processes or equipment; c) When the production of the newly trial-produced product or the normally- produced product is restored after suspension for 3 months; d) When there is a big difference between the exit-factory inspection and the last type inspection results; e) When the national quality supervision and inspection agency needs random inspection according to relevant requirements. 7.5 Decision rules 7.5.1 If there are 1 to 2 indicators in the inspection result fail, it shall take double quantity of samples from the same batch of products for re-inspection. Based on the re-inspection results, if there is one unqualified item, the entire batch of products are unqualified. ......
 
Source: Above contents are excerpted from the PDF -- translated/reviewed by: www.chinesestandard.net / Wayne Zheng et al.